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Volume 3 Issue 5
 
Volume & Issue: Volume 3 Issue 5

Palladium(II) complex with salicylaldehyde: Synthesis, characterization, crystal structure and thermal decomposition into PdO nano-particle
  Volume 3,Issue 5
 

Author :

Mehdi Ahmadi, Ahad Fasihizad, Barbara Machura, Rafael Kruszynski, Alireza Akbari, Tahere Barak

 

Abstract :

The synthesis and characterization of a palladium(II) complex containing two bidentate salicylaldehyde ligands is reported. The structure of the complex has been confirmed as squarer-planar by elemental analyses, molar conductivity measurement and spectroscopic analyses (IR and UV-Vis) as well as X-ray analysis. Thermal stability of the complex was studied by thermal gravimetric analysis (TGA), supplying palladium oxide as residue. The palladium oxide nono-sized has been also prepared by direct thermal composition of the complex. The nano-material was characterized by XRD powder diffraction.

 

Keywords :

Palladium, complex, X-Ray, TGA, Nano-material

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